Sealers and warm gutta-percha obturation techniques

J Endod. 2015 Jan;41(1):72-8. doi: 10.1016/j.joen.2014.06.007. Epub 2014 Aug 10.

Abstract

Introduction: Warm vertically compacted gutta-percha obturation techniques use root canal sealers that are heated during the obturation. This study aims at investigating the suitability of selected sealers with warm gutta-percha obturation techniques.

Methods: The composition of an experimental sealer (Septodont; Saint Maur-des-Fosses, France), MTA Fillapex (Angelus, Londrina, Brazil), Apexit Plus (Ivoclar, Schaan, Lichtenstein), and AH Plus (Dentsply International, Addlestone, UK) was assessed by scanning electron microscopic and energy-dispersive spectroscopic analysis. The effect of temperature during warm vertical compaction technique was investigated by testing the sealers' properties after 1 minute to 100°C or 37°C. The reaction products after setting were assessed by X-ray diffraction analysis and Fourier transform infrared spectroscopy. Changes in setting time, flow, and film thickness were determined using ISO 6876 (2012) specifications.

Results: The experimental tricalcium silicate-based sealer and Apexit Plus contained calcium hydroxide peaks after setting, which were absent in MTA Fillapex. The properties of AH Plus and the experimental sealer were modified by heat; the setting time was reduced, and film thickness increased. AH Plus had diminished N-H groups when heated to 100°C for 1 minute. MTA Fillapex, Septodont sealer, and Apexit Plus were unaffected by heat application.

Conclusions: The choice of sealer should be considered when selecting the obturation technique. The Septodont sealer is recommended for obturations using cold laterally condensed gutta-percha, whereas MTA Fillapex and Apexit Plus were suitable with warm gutta-percha obturation techniques.

Keywords: AH Plus; Apexit Plus; MTA Fillapex; Septodont experimental tricalcium silicate–based sealer; characterization; physical properties; root canal sealers; warm vertical compaction.

MeSH terms

  • Calcium Compounds / chemistry
  • Calcium Hydroxide / chemistry
  • Epoxy Resins / chemistry
  • Gutta-Percha / chemistry*
  • Hot Temperature
  • Materials Testing
  • Root Canal Filling Materials / chemistry*
  • Root Canal Obturation / methods*
  • Root Canal Preparation / methods
  • Silicates / chemistry
  • Spectroscopy, Fourier Transform Infrared
  • Surface Properties
  • X-Ray Diffraction
  • Zinc Oxide-Eugenol Cement / chemistry*

Substances

  • Apexit
  • Calcium Compounds
  • Epoxy Resins
  • Root Canal Filling Materials
  • Silicates
  • Zinc Oxide-Eugenol Cement
  • canals sealer
  • epoxy resin-based root canal sealer
  • tricalcium silicate
  • Gutta-Percha
  • Calcium Hydroxide