An in situ atomic force microscope for normal-incidence nanofocus X-ray experiments

J Synchrotron Radiat. 2016 Sep 1;23(Pt 5):1110-7. doi: 10.1107/S1600577516011437. Epub 2016 Aug 10.

Abstract

A compact high-speed X-ray atomic force microscope has been developed for in situ use in normal-incidence X-ray experiments on synchrotron beamlines, allowing for simultaneous characterization of samples in direct space with nanometric lateral resolution while employing nanofocused X-ray beams. In the present work the instrument is used to observe radiation damage effects produced by an intense X-ray nanobeam on a semiconducting organic thin film. The formation of micrometric holes induced by the beam occurring on a timescale of seconds is characterized.

Keywords: in situ atomic force microscopy; radiation damage; semiconducting organic thin films.

Publication types

  • Research Support, Non-U.S. Gov't