The purpose of this study was to evaluate the effect of calcium hydroxide [Ca(OH)2 ] on dentine composition and root fracture resistance. Root canals of fifty extracted mandibular premolars were prepared and divided into five groups (N = 10). Canals were filled with non-setting Ca(OH)2 or left empty and were subsequently stored in phosphate buffered saline for 7, 14, 30, or 90 days, respectively. Ca(OH)2 was then washed out, and roots were separated from the crowns and subjected to fracture strength test. Fractured fragments were examined by scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD). The results showed a significant and progressive reduction in fracture resistance the longer the duration of exposure to Ca(OH)2 , and the fracture resistance in teeth exposed for 90 days was significantly lower than in any other group. SEM revealed cracks in the dentine surfaces that had been exposed to Ca(OH)2 . FTIR showed a significantly lower mineral to matrix ratio in roots exposed to Ca(OH)2 for 30 and 90 days than seen in roots exposed for a shorter duration. XRD analysis revealed a reduction in dentine crystallinity. It was concluded that Ca(OH)2 significantly reduced the fracture resistance of the roots overtime. Exposure to Ca(OH)2 reduced the mineral to matrix ratio and crystallinity of the dentine.
Keywords: FTIR; XRD; calcium hydroxide; fracture resistance; root fracture.
© 2021 European Journal of Oral Sciences.