Bisphenol A release from an orthodontic adhesive and its correlation with the degree of conversion on varying light-curing tip distances

Am J Orthod Dentofacial Orthop. 2011 Aug;140(2):239-44. doi: 10.1016/j.ajodo.2010.02.037.

Abstract

Introduction: The aims of this research were to use high-performance liquid chromatography to assess the bisphenol A (BPA) released from an orthodontic adhesive (Transbond XT; 3M Unitek, Monrovia, Calif) with various light-curing tip distances and to correlate the release to the degree of conversion.

Methods: One hundred thirty-eight premolar brackets were divided into 3 groups of 40 each for the high-performance liquid chromatography analysis and 3 groups of 6 each for assessing the degree of conversion. Fourier transform infrared spectroscopy was used for this purpose. Each group was studied at light-curing tip distances of 0, 5, and 10 mm. Statistical analyses were performed by using 2-way analysis of variance (ANOVA), post-hoc multiple comparisons Tukey HSD tests, and paired t tests. Pearson correlation was used to assess the correlation between the degree of conversion and BPA release.

Results: BPA release was greater in specimens cured with a greater light-curing tip distance. The degree of conversion decreased with increased light-curing tip distances. A negative correlation was found between BPA release and degree of conversion.

Conclusions: Clinicians should ensure that the adhesive is completely cured by keeping the light-curing tip as close to the adhesive as clinically possible.

MeSH terms

  • Analysis of Variance
  • Benzhydryl Compounds
  • Chromatography, High Pressure Liquid
  • Hardness
  • Light-Curing of Dental Adhesives / methods*
  • Materials Testing
  • Orthodontic Brackets
  • Phenols / analysis*
  • Polymerization
  • Resin Cements / chemistry*
  • Resin Cements / radiation effects
  • Spectroscopy, Fourier Transform Infrared
  • Statistics, Nonparametric

Substances

  • Benzhydryl Compounds
  • Phenols
  • Resin Cements
  • Transbond XT
  • bisphenol A