Efficacy of surface treatments on the bond strength of resin cements to two brands of zirconia ceramic

J Adhes Dent. 2013 Jun;15(3):259-67. doi: 10.3290/j.jad.a28729.

Abstract

Purpose: To compare the shear bond strengths (SBS) of two cements to two Y-TZP ceramics subjected to different surface treatments.

Materials and methods: Zirconia specimens were made from Lava (n = 36) and IPS e.max ZirCAD (n = 36), and their surfaces were treated as follows: no treatment (control), silica coating with 30-µm silica-modified alumina (Al2O3) particles (CoJet Sand), or coating with liners Lava Ceram for Lava and Intensive ZirLiner for IPS e.max ZirCAD. Composite resin cylinders were bonded to zirconia with Panavia F or RelyX Unicem resin cements. All specimens were thermocycled (6000 cycles at 5°C/55°C) and subjected to SBS testing. Data were analyzed by three-way ANOVA and Tukey's (HSD) post-hoc test (α = 0.05). Failure mode was analyzed by stereomicroscope and SEM.

Results: CoJet Sand and liners promoted significantly higher SBS than their control groups, but had similar results to one another. Panavia F provided significantly higher SBS values than RelyX Unicem (p < 0.01) for nontreated zirconia specimens of both brands. When Lava and IPS e.max ZirCAD were abraded with CoJet Sand, RelyX Unicem promoted significantly higher SBS values than Panavia F (p < 0.001). There was no significant difference between the two cements when the zirconia specimens were treated with their respective liners. The nontreated specimens and those treated with CoJet Sand exhibited a high percentage of adhesive and mixed A failures, while the specimens treated with liners presented an increase in mixed A and mixed C failures as well as some cohesive failure in the bulk of Lava Ceram for both cements.

Conclusion: CoJet Sand and liners provided the best surface treatment for Lava and IPS e.max ZirCAD. The best surface treatment/cement combinations were CoJet Sand/RelyX Unicem and liner/Panavia F. SBS of Panavia F and RelyX Unicem was not influenced by the zirconia brand.

Publication types

  • Comparative Study
  • Randomized Controlled Trial

MeSH terms

  • Adhesiveness
  • Aluminum Oxide / chemistry
  • Aluminum Silicates / chemistry
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Cements / chemistry
  • Dental Etching / methods
  • Dental Materials / chemistry*
  • Glass / chemistry
  • Humans
  • Humidity
  • Materials Testing
  • Methacrylates / chemistry
  • Microscopy, Electron, Scanning
  • Resin Cements / chemistry*
  • Shear Strength
  • Silicon Dioxide / chemistry
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Time Factors
  • Yttrium / chemistry*
  • Zirconium / chemistry*

Substances

  • Aluminum Silicates
  • Composite Resins
  • Dental Cements
  • Dental Materials
  • ED Primer II
  • Methacrylates
  • Monobond S
  • Panavia-Fluoro
  • Rely X Unicem
  • Resin Cements
  • Scotchbond Multi-Purpose
  • Z100 composite resin
  • yttria stabilized tetragonal zirconia
  • Clearfil Photo Bond
  • Yttrium
  • Silicon Dioxide
  • Zirconium
  • Aluminum Oxide