Effects of Temperature and Aging on Working/Setting Time of Dual-cured Resin Cements

Oper Dent. 2015 Nov-Dec;40(6):E222-9. doi: 10.2341/13-361-L. Epub 2015 Jul 7.

Abstract

Objectives: To evaluate the effects of aging and temperature on working time (WT) and setting time (ST) of several dual-cured resin cements.

Methods: WT and ST were determined with a thermo-controlled stage oscillating rheometer. New cement kits were used for the study. Cements were mixed according to instructions and dispensed on the oscillating stage that was preset at 22°C or 37°C. Rheologic charts were generated from the beginning of mixing until no further oscillation was detected. After initial measurements, cement kits were aged at 37°C for 12 weeks, and WT/ST was determined again at both temperatures. Five samples were read for each material and condition. Data were analyzed with repeated measures analysis of variance and a Tukey test at α=5% for each individual material.

Results: The WT and ST of all cements were significantly affected by temperature and aging (p<0.05). In general, higher temperature accelerated WT/ST, but aging effects were material dependent. Some materials presented reduced WT/ST, whereas others showed increased WT/ST, regardless of the temperature.

Conclusions: The WT and ST were significantly affected by temperature variation and aging condition. Although temperature changes appeared to affect all materials similarly, aging effects were material dependent.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Materials Testing*
  • Resin Cements / chemistry*
  • Rheology
  • Temperature*
  • Time Factors

Substances

  • DCR cement
  • Resin Cements